Achieving robust processes via three experiment-design options (part 1)
The goal of robustness studies is to demonstrate that our processes will be successful upon implementation in the field when they are exposed to anticipated noise factors. There are several assumptions and underlying concepts that need to be understood when setting out to conduct a robustness study.
First, it is necessary that the noise factors be identified and can be controlled during the robustness study itself. Noise factors that cannot be controlled, cannot be evaluated. They will merely serve to increase variation within the study and exacerbate the unexplained variation encountered, i.e., they increase the residual (error) term.
Second, it is necessary to consider the type of noise variation being studied. Our modeling will be built upon X’s – the factors we control within our process, and Z’s – noise factors external to our system that we (eventually) cannot control. Variation around the chosen set points for X factors creates one source of noise that influences our responses (Y’s). Variation of identified external noise (Z’s) creates another source of influence. These Z factors, however, do not have a “set point.” In the field, they randomly appear and cause variation upon process responses.
Some DOE experts differentiate the two groups of terms (variation in X’s versus variation in Z’s) by using the terms robustness for stability against X-factor variation, and ruggedness to express stability against Z-factor variation. That differentiation is not universally used and nowadays the term ruggedness is less common, so I will refer to both concepts under the umbrella term, “robust design.”
Carefully considering these principles, three distinct types of designs emerge that address robustness:
I. Having settled on process settings, we desire to demonstrate the system is insensitive to external noise-factor variation, i.e., robust against Z factor influence.
II. Given we may have variation between our selected process settings and the actual factor conditions that may be seen in the field, we wish to find settings that are insensitive to this variation. In other words, we may set our controlled X factors, but these factors wander from their set points and cause variation in our results. Our goal is to achieve our desired Y values while minimizing the variation stemming from imperfect process factor control. The impact of external noise factors (Z’s) is not explored in this type of study.
III. Given a system having controllable factors (X’s) and non-controllable noise factors (Z’s) impacting one or more desirable properties (Y’s), we wish to find the ideal settings for the controllable factors that simultaneously maximize the properties of interest, while minimizing the impact of variation from both types of noise factors.
DOE tools for the first type of robustness study are discussed below, with more to come in future blog posts.
Design-Type I: Robustness against external noise factors
Here, we aim to prove that our process is robust against expected noise factors due to field conditions. For example, we may settle on baking conditions for making bread, but we now wish to demonstrate that anticipated changes in ambient temperature, ambient humidity, and flour brand do not impact the rise height of the bread.
The first thing we need to ask ourselves is our threshold of acceptance. Do we care about 0.1 mm of rise height? Or perhaps anything under 10 mm (1cm) change from baseline is inconsequential. Whatever value we settle on is our response change delta (ΔY) of interest – the amount of noise factor impact deemed to be alarming. If the actual noise factor causes a change less than that value, we accept that we may not detect it in this DOE.
We also need some assessment of the natural variation in the system, i.e., how much variation in results seen when repeatedly running the same conditions. This is our standard deviation sigma (σ) Note that this value would be reported in the fit statistics if a prior DOE had been run on this system (generally the case prior to doing a robustness study).
For this type of robustness study, a resolution III two-level factorial design suffices, provided we have sufficient Power (>80%) in the design, which is driven by the delta to sigma ratio (ΔY/σ). Power is the probability of detecting an effect of the chosen ΔY value, if indeed it exists. (Stat-Ease software conveniently calculates power when you construct factorial experiments using its design wizard.) If we do not have sufficient power, then more runs must be done—the best option being an upgrade to a resolution IV design. Due to their greater flexibility for number of runs, Plackett-Burman designs are another commonly used resolution III template for these types of robustness studies.
The hope of course is that we find nothing of significance, i.e., none of the noise factors cause the response to change by more than our chosen ΔY. That would be the goal of this type of robustness DOE.
If we do see noise factors appearing as significant, we have a dilemma: a resolution III experiment won’t reveal if the indicated factor is responsible, or if we really have an interaction between two other factors that is the culprit. All we will know for sure is that the system is NOT robust against the noise factors we have evaluated, at least at the selected value for ΔY. Note, however, that if we ran a Resolution IV DOE, we would have greater confidence that the indicated noise factor was the cause. But we really can’t be certain of that conclusion with anything less than a Resolution V experiment.
It is for this reason that we do not recommend using a Resolution III experiment for anything other than this type of robustness evaluation where we merely wish to prove our process is insensitive to external noise factors.
For additional information, see Mark Anderson’s 2021 webinar on DOE for Ruggedness Testing.
Look forward to parts 2 and 3 of this series, coming out in April and covering the other two design scenarios.